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A new reagent for a very simple and efficient determination of enantiomeric purity of alcohols by 31P NMR |
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Published in | Tetrahedron: Asymmetry. 1990, vol. 1, no. 7, p. 437-440 | |
Abstract | A new reagent is described for the determination of enantiomeric excess of chiral alcohols. This derivatizing agent allows an accurate analysis by 31P NMR. A large array of primary, secondary, and tertiary alcohols, functionalized or not, were successfully tested. Reagent 7 is easy to prepare and reacts alone with the chiral alcohol, at room temperature, eventually directly in the NMR tube. | |
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Citation (ISO format) | ALEXAKIS, Alexandre et al. A new reagent for a very simple and efficient determination of enantiomeric purity of alcohols by 31P NMR. In: Tetrahedron: Asymmetry, 1990, vol. 1, n° 7, p. 437-440. doi: 10.1016/S0957-4166(00)86347-8 https://archive-ouverte.unige.ch/unige:8180 |