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Title

A new reagent for a very simple and efficient determination of enantiomeric purity of alcohols by 31P NMR

Authors
Mutti, Stephane
Normant, Jean F.
Mangeney, Pierre
Published in Tetrahedron: Asymmetry. 1990, vol. 1, no. 7, p. 437-440
Abstract A new reagent is described for the determination of enantiomeric excess of chiral alcohols. This derivatizing agent allows an accurate analysis by 31P NMR. A large array of primary, secondary, and tertiary alcohols, functionalized or not, were successfully tested. Reagent 7 is easy to prepare and reacts alone with the chiral alcohol, at room temperature, eventually directly in the NMR tube.
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ALEXAKIS, Alexandre et al. A new reagent for a very simple and efficient determination of enantiomeric purity of alcohols by 31P NMR. In: Tetrahedron: Asymmetry, 1990, vol. 1, n° 7, p. 437-440. https://archive-ouverte.unige.ch/unige:8180

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Deposited on : 2010-06-21

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