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Ultrasound assisted cleavage of hydrazines by Raney nickel

Lensen, Nathalie
Mangeney, Pierre
Published in Synlett. 1991, no. 9, p. 625-626
Abstract The reductive N-N cleavage of N-substituted N',N'-dimethylhydrazines to give primary amines by Raney nickel/hydrogen is conveniently performed under atmospheric pressure of hydrogen by sonication of the reaction vessel in a simple ultrasound cleaner. Sterically hindered hydrazines are also cleaved and no racemization or debenzylation is observed.
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ALEXAKIS, Alexandre, LENSEN, Nathalie, MANGENEY, Pierre. Ultrasound assisted cleavage of hydrazines by Raney nickel. In: Synlett, 1991, n° 9, p. 625-626.

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Deposited on : 2010-06-21

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