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Mild protection and deprotection of alcohols as ter-butyl ethers in the field of pheromone synthesis

Authors
Gardette, M.
Colin, S.
Published in Tetrahedron Letters. 1988, vol. 29, no. 24, p. 2951-2954
Abstract α,ω-Halohydrins and Ω-acetylenic alcohols are protected as t-butyl ethers by reaction with isobutene and an acid catalyst : Amberlyst H-15. t-Butyl ethers are, in turn, cleaved to acetates by Ac2O and 10% FeCl3 in Et2O solvent. Under these mild conditions conjugated dienic systems are neither destroyed nor isomerized.
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ALEXAKIS, Alexandre, GARDETTE, M., COLIN, S. Mild protection and deprotection of alcohols as ter-butyl ethers in the field of pheromone synthesis. In: Tetrahedron Letters, 1988, vol. 29, n° 24, p. 2951-2954. https://archive-ouverte.unige.ch/unige:8072

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Deposited on : 2010-06-21

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