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Title

An easy and fast way to determine the enantiomeric purity of substituted cyclanones

Authors
Frutos, Juan C.
Mangeney, Pierre
Published in Tetrahedron: Asymmetry. 1993, vol. 4, no. 12, p. 2431-2434
Abstract The determination of the enantiomeric purity of 2 or 3-substituted cyclanones, particularly cyclohexanones, is conveniently achieved by derivatisation into cyclic aminals with commercially available (R, R)-1,2-diphenylethylenediamine. The derivatisation procedure is directly done into the NMR tube, instantaneously, and 13C NMR allows an accurate measure of the ee.
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ALEXAKIS, Alexandre, FRUTOS, Juan C., MANGENEY, Pierre. An easy and fast way to determine the enantiomeric purity of substituted cyclanones. In: Tetrahedron: Asymmetry, 1993, vol. 4, n° 12, p. 2431-2434. https://archive-ouverte.unige.ch/unige:8062

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Deposited on : 2010-06-21

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