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Synthesis of Spiro Ketals, Orthoesters, and Orthocarbonates by CpRu-Catalyzed Decomposition of α-Diazo-β-ketoesters

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Published in Organic Letters. 2016, vol. 18, no. 3, p. 240-243
Abstract Reactions of α-diazo-β-ketoesters with cyclic ketones, lactones, and carbonates are reported. Thanks to the combined use of salt [CpRu(CH3CN)3][BArF] and 1,10-phenanthroline as catalyst for the diazo decomposition, effective and practical syntheses of spiro bicyclic ketals, orthoesters, and orthocarbonates are afforded.
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Research group Groupe Lacour
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TORTORETO, Cecilia et al. Synthesis of Spiro Ketals, Orthoesters, and Orthocarbonates by CpRu-Catalyzed Decomposition of α-Diazo-β-ketoesters. In: Organic Letters, 2016, vol. 18, n° 3, p. 240-243. https://archive-ouverte.unige.ch/unige:79450

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Deposited on : 2016-01-18

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