Doctoral thesis
OA Policy
English

From 2D to 1D homodecoupled high-resolution proton NMR

ContributorsCotte, Axelle
Defense date2015-02-13
Abstract

The existence of extended homonuclear coupling structures causes signal overlaps in 1D and 2D proton spectra. Numerous techniques have been developed through years to reduce multiplet patterns into singlets. A new approach is proposed here. The combination of a 2D experiment decoupled in the F1 dimension - by the introduction of a homodecoupling element in the evolution time - with spectral aliasing and frequency modulation of pulses leads to the obtention of 1D homodecoupled proton spectra with enhanced spectral resolution and sensitivity.

Keywords
  • NMR
  • Proton
  • Homodecoupling
  • High-resolution
Citation (ISO format)
COTTE, Axelle. From 2D to 1D homodecoupled high-resolution proton NMR. Doctoral Thesis, 2015. doi: 10.13097/archive-ouverte/unige:75760
Main files (1)
Thesis
accessLevelPublic
Identifiers
1101views
411downloads

Technical informations

Creation30/09/2015 20:41:00
First validation30/09/2015 20:41:00
Update time14/03/2023 23:40:11
Status update14/03/2023 23:40:10
Last indexation31/10/2024 01:26:37
All rights reserved by Archive ouverte UNIGE and the University of GenevaunigeBlack