en
Doctoral thesis
Open access
English

From 2D to 1D homodecoupled high-resolution proton NMR

ContributorsCotte, Axelle
Defense date2015-02-13
Abstract

The existence of extended homonuclear coupling structures causes signal overlaps in 1D and 2D proton spectra. Numerous techniques have been developed through years to reduce multiplet patterns into singlets. A new approach is proposed here. The combination of a 2D experiment decoupled in the F1 dimension - by the introduction of a homodecoupling element in the evolution time - with spectral aliasing and frequency modulation of pulses leads to the obtention of 1D homodecoupled proton spectra with enhanced spectral resolution and sensitivity.

eng
Keywords
  • NMR
  • Proton
  • Homodecoupling
  • High-resolution
Citation (ISO format)
COTTE, Axelle. From 2D to 1D homodecoupled high-resolution proton NMR. 2015. doi: 10.13097/archive-ouverte/unige:75760
Main files (1)
Thesis
accessLevelPublic
Identifiers
959views
293downloads

Technical informations

Creation2015/09/30 20:41:00
First validation2015/09/30 20:41:00
Update time2023/03/14 23:40:11
Status update2023/03/14 23:40:10
Last indexation2024/01/29 20:33:31
All rights reserved by Archive ouverte UNIGE and the University of GenevaunigeBlack