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From 2D to 1D homodecoupled high-resolution proton NMR

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Defense Thèse de doctorat : Univ. Genève, 2015 - Sc. 4785 - 2015/02/13
Abstract The existence of extended homonuclear coupling structures causes signal overlaps in 1D and 2D proton spectra. Numerous techniques have been developed through years to reduce multiplet patterns into singlets. A new approach is proposed here. The combination of a 2D experiment decoupled in the F1 dimension - by the introduction of a homodecoupling element in the evolution time - with spectral aliasing and frequency modulation of pulses leads to the obtention of 1D homodecoupled proton spectra with enhanced spectral resolution and sensitivity.
Keywords NMRProtonHomodecouplingHigh-resolution
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URN: urn:nbn:ch:unige-757601
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COTTE, Axelle. From 2D to 1D homodecoupled high-resolution proton NMR. Université de Genève. Thèse, 2015. https://archive-ouverte.unige.ch/unige:75760

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Deposited on : 2015-10-05

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