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Synthesis of {323}-p-Octiphenyls: Orthogonal Functionalization along a Rigid-Rod Scaffold for Refined Supramolecular Architecture

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Published in Organic Letters. 2004, vol. 6, no. 6, p. 885-887
Abstract The synthesis of p-octiphenyls carrying orthogonal tert-butyl esters in the peripheral positions 1(2), 2(2), 3(3), 6(2), 7(3), and 8(2) and either p-methoxybenzyl or benzyl ester substituents in the central positions 4(2) and 5(3) is described. Resolution-enhanced HSQC/HMBC two-dimensional NMR spectroscopy is implemented as an attractive method for the complete characterization of complex p-oligophenyl scaffolds.
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PMID: 15012056
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RONAN, Dawn et al. Synthesis of {323}-p-Octiphenyls: Orthogonal Functionalization along a Rigid-Rod Scaffold for Refined Supramolecular Architecture. In: Organic Letters, 2004, vol. 6, n° 6, p. 885-887. https://archive-ouverte.unige.ch/unige:6962

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Deposited on : 2010-06-18

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