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One-Step Stereoselective Synthesis and NMR Chiral Shift Properties of a Novel Hexacoordinated Phosphorus Cation

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Published in Organic Letters. 2002, vol. 4, no. 14, p. 2309-2312
Abstract Tropolone, binol, and PCl(5) react in CH(2)Cl(2) at reflux to generate in one step a novel C(2)-symmetric hexacoordinated phosphorus cation of configuration controlled by the binol ligand. It behaves as an efficient NMR chiral shift agent for chiral anionic phosphate and borate anions.
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PMID: 12098234
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LACOUR, Jérôme, VIAL, Laurent, BERNARDINELLI, Gérald Hugues. One-Step Stereoselective Synthesis and NMR Chiral Shift Properties of a Novel Hexacoordinated Phosphorus Cation. In: Organic Letters, 2002, vol. 4, n° 14, p. 2309-2312. https://archive-ouverte.unige.ch/unige:6958

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Deposited on : 2010-06-18

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