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One-Step Synthesis of Nitrogen-Containing Medium-Sized Rings via α-Imino Diazo Intermediates

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Published in Organic Letters. 2014, vol. 16, no. 12, p. 3232-3235
Abstract Eight- and 9-membered dioxazocines and dioxazonines are readily synthesized starting from N-sulfonyl-1,2,3-triazoles in a single-step procedure. A perfect regioselectivity and generally good yields (up to 92%) are obtained under dirhodium catalysis using 1,3-dioxolane and 1,3-dioxane as solvents and reagents.
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MEDINA, Florian, BESNARD, Céline, LACOUR, Jérôme. One-Step Synthesis of Nitrogen-Containing Medium-Sized Rings via α-Imino Diazo Intermediates. In: Organic Letters, 2014, vol. 16, n° 12, p. 3232-3235. https://archive-ouverte.unige.ch/unige:37985

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Deposited on : 2014-06-20

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