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NMR pulse sequence developments for high resolution in heteronuclear 2d experiments

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Defense Thèse de doctorat : Univ. Genève, 2012 - Sc. 4525 - 2012/12/03
Abstract Low resolution in the indirect dimension of 1H–13C heteronuclear experiments is a long-standing problem of NMR spectroscopy, which has not found a satisfactory solution. Among the numerous techniques aiming at increasing the resolution of the indirect dimension of 2D NMR spectra, we focused on spectral aliasing, which plays a unique role for its simplicity of application and efficiency. We also developed a homonuclear 13C decoupling in the F1 dimension, which enhances sensitivity and resolution by transforming the spread of multiplet patterns of carbons into singlets when samples with 13C labeling are involved.
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URN: urn:nbn:ch:unige-369844
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FOROOZANDEH, Mohammadali. NMR pulse sequence developments for high resolution in heteronuclear 2d experiments. Université de Genève. Thèse, 2012. https://archive-ouverte.unige.ch/unige:36984

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Deposited on : 2014-05-28

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