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NQR studies of polyhalocuprate(I) anions

Ramaprabhu, Sundara
Ferretti, Rachel
Published in Inorganica Chimica Acta. 1994, vol. 227, no. 1, p. 153-157
Abstract Attempts to prepare the tricyclohexylphosphine or triphenylstibine analogues of the recently reported (triphenylphosphine) CuX2− anions were unsuccessful and instead resulted in the formation of a variety of polyhalocuprate anions. The structure of one of these, [CH3P(C6H5)3]2Cu2I4, has been determined; monoclinic, P21/c; a = 16.715(3), b = 10.787(2), c = 23.196(3) Å, β=98.59(1)°, Z=4; R=6.3%, Rw=3.1%. The 63Cu NQR spectra of twelve such polyhalocuprate anions were observed and the results compared with those of previously reported polyhalocuprates.
Keywords Crystal structuresCopper complexesHalide complexesAnion complexes
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Research group Groupe Lucken
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RAMAPRABHU, Sundara et al. NQR studies of polyhalocuprate(I) anions. In: Inorganica Chimica Acta, 1994, vol. 227, n° 1, p. 153-157. https://archive-ouverte.unige.ch/unige:2876

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Deposited on : 2009-09-21

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