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Scientific article
English

Broadband 13C-Homodecoupled Heteronuclear Single-Quantum Correlation Nuclear Magnetic Resonance

Published inChemPhysChem, vol. 12, no. 13, p. 2409-2411
Publication date2011
Abstract

13C-homodecoupling in F1: Eliminating homonuclear 13C scalar couplings is a challenging NMR problem when enriched compounds are studied by NMR. The 13C-homodecoupled heteronuclear single-quantum correlation (HSQC) experiment (BBHD-HSQC) relies on the Zangger–Sterk pulse sequence element to combine spatial encoding of the chemical shift with the refocusing of couplings. The sequence is applied to fully enriched 13C cholesterol.

Keywords
  • Broadband homodecoupling
  • Cholesterol
  • Isotopes
  • NMR spectroscopy
  • Spatial encoding
Citation (ISO format)
FOROOZANDEH, Mohammadali, GIRAUDEAU, Patrick, JEANNERAT, Damien. Broadband 13C-Homodecoupled Heteronuclear Single-Quantum Correlation Nuclear Magnetic Resonance. In: ChemPhysChem, 2011, vol. 12, n° 13, p. 2409–2411. doi: 10.1002/cphc.201100411
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ISSN of the journal1439-4235
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Technical informations

Creation09/06/2011 6:01:00 PM
First validation09/06/2011 6:01:00 PM
Update time03/14/2023 4:54:01 PM
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