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New trialkylsilyl enol ether chemistry: new regiospecific methodology for the synthesis of α,β-unsaturated cyclic ketones

Authors
Magnus, Philip
Evans, Andrew
Published in Tetrahedron Letters. 1992, vol. 33, no. 21, p. 2933 - 2936
Abstract Treatment of TIPS enol ethers with PhIO/TMSN3 followed by desilylation/elimination with fluoride ion gives good yields of the a,ß-unsaturated ketone. Treatment of triisopropylsilyl enol ethers with PhIO/TMSN3 followed by fluoride ion gives good yields of the a,ß-unsaturated ketone.
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MAGNUS, Philip, EVANS, Andrew, LACOUR, Jérôme. New trialkylsilyl enol ether chemistry: new regiospecific methodology for the synthesis of α,β-unsaturated cyclic ketones. In: Tetrahedron Letters, 1992, vol. 33, n° 21, p. 2933 - 2936. https://archive-ouverte.unige.ch/unige:6608

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Deposited on : 2010-05-17

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