Broadband 13C-Homodecoupled Heteronuclear Single-Quantum Correlation Nuclear Magnetic Resonance

Foroozandeh, Mohammadali; Giraudeau, Patrick; Jeannerat, Damien

doi:10.1002/cphc.201100411

Scientific article

English

Broadband 13C-Homodecoupled Heteronuclear Single-Quantum Correlation Nuclear Magnetic Resonance

ContributorsForoozandeh, Mohammadali; Giraudeau, Patrick; Jeannerat, Damien

Published inChemPhysChem, vol. 12, no. 13, p. 2409-2411

Publication date2011

Abstract

13C-homodecoupling in F1: Eliminating homonuclear 13C scalar couplings is a challenging NMR problem when enriched compounds are studied by NMR. The 13C-homodecoupled heteronuclear single-quantum correlation (HSQC) experiment (BBHD-HSQC) relies on the Zangger–Sterk pulse sequence element to combine spatial encoding of the chemical shift with the refocusing of couplings. The sequence is applied to fully enriched 13C cholesterol.

Keywords

Broadband homodecoupling
Cholesterol
Isotopes
NMR spectroscopy
Spatial encoding

Affiliation entities

Faculté des sciences / Section de chimie et biochimie / Département de chimie organique

Citation (ISO format)

FOROOZANDEH, Mohammadali, GIRAUDEAU, Patrick, JEANNERAT, Damien. Broadband 13C-Homodecoupled Heteronuclear Single-Quantum Correlation Nuclear Magnetic Resonance. In: ChemPhysChem, 2011, vol. 12, n° 13, p. 2409–2411. doi: 10.1002/cphc.201100411

Article (Published version)

Identifiers

PID : unige:16898
DOI : 10.1002/cphc.201100411

Journal ISSN1439-4235

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Creation06/09/2011 18:01:00

First validation06/09/2011 18:01:00

Update time14/03/2023 16:54:01

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Broadband 13C-Homodecoupled Heteronuclear Single-Quantum Correlation Nuclear Magnetic Resonance

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